{"id":2736,"date":"2015-04-10T12:40:00","date_gmt":"2015-04-10T12:40:00","guid":{"rendered":"https:\/\/chempublishers.com\/pjc\/?p=2736"},"modified":"2025-06-14T05:26:30","modified_gmt":"2025-06-14T05:26:30","slug":"pjc-0215","status":"publish","type":"post","link":"https:\/\/chempublishers.com\/Pakistan-journal-of-chemistry\/2015\/04\/10\/pjc-0215\/","title":{"rendered":"Kinetics and Mechanism of Reduction of Fe (III)-Acetohydroxamic Acid by Hydroxylamine Hydrochloride at Acidic pH"},"content":{"rendered":"\t\t<div data-elementor-type=\"wp-post\" data-elementor-id=\"2736\" class=\"elementor elementor-2736\" data-elementor-post-type=\"post\">\n\t\t\t\t<div class=\"elementor-element elementor-element-c09084a e-flex e-con-boxed e-con e-parent\" data-id=\"c09084a\" data-element_type=\"container\">\n\t\t\t\t\t<div class=\"e-con-inner\">\n\t\t<div class=\"elementor-element elementor-element-5b22c51 e-con-full e-flex e-con e-child\" data-id=\"5b22c51\" data-element_type=\"container\">\n\t\t\t\t<div class=\"elementor-element elementor-element-6688d12 elementor-widget elementor-widget-text-editor\" data-id=\"6688d12\" data-element_type=\"widget\" data-widget_type=\"text-editor.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t\t\t\t\t<table border=\"0\" width=\"100%\" cellspacing=\"0\" cellpadding=\"0\" align=\"center\"><tbody><tr><td><div><strong>Research Article | Open Access<\/strong><\/div><div class=\"item doi\"><span class=\"value\">Volume 5 | Issue 1 |\u00a0<a href=\"https:\/\/chempublishers.com\/Pakistan-journal-of-chemistry\/wp-content\/uploads\/sites\/2\/2024\/12\/PJC-v05.i01.p02.pdf\" target=\"_blank\" rel=\"noopener\">https:\/\/doi.org\/10.15228\/2015.v05.i01.p02<\/a><\/span><\/div><\/td><\/tr><\/tbody><\/table><h4>Kinetics and Mechanism of Reduction of Fe (III)-Acetohydroxamic Acid by Hydroxylamine Hydrochloride at Acidic pH<\/h4><h4><strong><b>M. Hassan<\/b><\/strong><\/h4><p>Department of Chemistry, University of Karachi, Karachi, Pakistan.<\/p><h4><strong><b>S. Nisar<\/b><\/strong><\/h4><p>Department of Chemistry, University of Karachi, Karachi, Pakistan.<\/p><h4><strong><b>S. A. Kazmi<\/b><\/strong><\/h4><p>Department of Chemistry, University of Karachi, Karachi, Pakistan.<\/p><h4><strong><b>M. Qadri<\/b><\/strong><\/h4><p>Department of Chemistry, University of Karachi, Karachi, Pakistan.<\/p><h4><strong><b>S. Imad<\/b><\/strong><\/h4><p>Chemical Metrology Division, National Physical and Standard Laboratory (PCSIR), Islamabad. Pakistan.<\/p><h4><strong><b>R. Naz<\/b><\/strong><\/h4><p>Department of Chemistry, University of Karachi, Karachi, Pakistan.<\/p><table border=\"0\" width=\"93%\" cellspacing=\"0\" cellpadding=\"0\" align=\"center\"><tbody><tr><td align=\"center\" valign=\"top\"><strong>Received<\/strong><br \/>06 Mar, 2015<\/td><td align=\"center\" valign=\"top\"><strong>Accepted<\/strong><br \/>21 Sep, 2015<\/td><td align=\"center\" valign=\"top\"><strong>Published<\/strong><br \/>06 Dec, 2015<\/td><\/tr><\/tbody><\/table><p><strong><u><b>ABSTRACT:<\/b><\/u><\/strong><\/p><p>The complexes of Fe(III)-AHA were prepared in acetate buffer of pH 4.5, 5.0 and 5.5. Stopped flow technique was used to study the reduction of these complexes by hydroxylamine hydrochloride. The reaction shows a biphasic behavior which is significantly pH dependent. Rate of both phases increases with hydrogen ion concentration. The rate was found to be first order with respect to [Fe(III)]. The overall rate was neither first order nor second order but there was a pre-equilibrium in mechanism. Slight increase in the values of kobs might be a consequence of increased reducing power of hydroxylamine hydrochloride with pH.<\/p><h3><strong><b>How to Cite this paper?<\/b><\/strong><\/h3><p><strong><b>APA-7 Style<\/b><\/strong><br \/>Hassan, M., Nisar, S., Kazmi, S. A., Qadri, M., Imad, S., &amp; Naz, R. (2015). Kinetics and Mechanism of Reduction of Fe (III)-Acetohydroxamic Acid by Hydroxylamine Hydrochloride at Acidic pH.\u00a0<em><i>Pakistan Journal of Chemistry<\/i><\/em>,\u00a0<em><i>5<\/i><\/em>(1). https:\/\/doi.org\/10.15228\/2015.v05.i01.p02<\/p><p><strong><b>ACS Style<\/b><\/strong><br \/>Hassan, M., Nisar, S., Kazmi, S.A., Qadri, M., Imad, S. and Naz, R., 2015. Kinetics and Mechanism of Reduction of Fe (III)-Acetohydroxamic Acid by Hydroxylamine Hydrochloride at Acidic pH.\u00a0<em><i>Pakistan Journal of Chemistry<\/i><\/em>,\u00a0<em><i>5<\/i><\/em>(1). https:\/\/doi.org\/10.15228\/2015.v05.i01.p02<\/p><p><strong><b>AMA Style<\/b><\/strong><br \/>Hassan M, Nisar S, Kazmi SA, Qadri M, Imad S, Naz R. Kinetics and Mechanism of Reduction of Fe (III)-Acetohydroxamic Acid by Hydroxylamine Hydrochloride at Acidic pH. Pakistan Journal of Chemistry. 2015 Mar 1;5(1). https:\/\/doi.org\/10.15228\/2015.v05.i01.p02<\/p><p><strong><b>Chicago\/Turabian Style<\/b><\/strong><br \/>Hassan, M., S. Nisar, S. A. Kazmi, M. Qadri, S. Imad, and R. Naz. &#8220;Kinetics and Mechanism of Reduction of Fe (III)-Acetohydroxamic Acid by Hydroxylamine Hydrochloride at Acidic pH.&#8221;\u00a0<em><i>Pakistan Journal of Chemistry<\/i><\/em>\u00a05, no. 1 (2015). https:\/\/doi.org\/10.15228\/2015.v05.i01.p02<\/p><p><a href=\"https:\/\/creativecommons.org\/licenses\/by\/4.0\/\" rel=\"license\"><img decoding=\"async\" src=\"https:\/\/i.creativecommons.org\/l\/by\/4.0\/88x31.png\" alt=\"Creative Commons License\" \/><\/a><\/p><p>This work is licensed under a\u00a0<a href=\"https:\/\/creativecommons.org\/licenses\/by\/4.0\/\" rel=\"license\">Creative Commons Attribution 4.0 International License<\/a>.<\/p>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t<div class=\"elementor-element elementor-element-d3180c9 e-con-full e-flex e-con e-child\" data-id=\"d3180c9\" data-element_type=\"container\">\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t","protected":false},"excerpt":{"rendered":"<p>Research Article | Open AccessVolume 5 | Issue 1 |\u00a0https:\/\/doi.org\/10.15228\/2015.v05.i01.p02 Kinetics and Mechanism of Reduction of Fe (III)-Acetohydroxamic Acid by Hydroxylamine Hydrochloride at Acidic pH M. Hassan Department of Chemistry, University of Karachi, Karachi, Pakistan. S. Nisar Department of Chemistry, University of Karachi, Karachi, Pakistan. S. A. Kazmi Department of Chemistry, University of Karachi, Karachi, [&hellip;]<\/p>\n","protected":false},"author":2,"featured_media":0,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"_acf_changed":false,"footnotes":""},"categories":[1],"tags":[],"class_list":["post-2736","post","type-post","status-publish","format-standard","hentry","category-uncategorized"],"acf":[],"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v25.1 - https:\/\/yoast.com\/wordpress\/plugins\/seo\/ -->\n<title>Kinetics and Mechanism of Reduction of Fe (III)-Acetohydroxamic Acid by Hydroxylamine Hydrochloride at Acidic pH - Pakistan Journal of Chemistry<\/title>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/chempublishers.com\/Pakistan-journal-of-chemistry\/2015\/04\/10\/pjc-0215\/\" \/>\n<meta property=\"og:locale\" content=\"en_US\" \/>\n<meta property=\"og:type\" content=\"article\" \/>\n<meta property=\"og:title\" content=\"Kinetics and Mechanism of Reduction of Fe (III)-Acetohydroxamic Acid by Hydroxylamine Hydrochloride at Acidic pH - Pakistan Journal of Chemistry\" \/>\n<meta property=\"og:description\" content=\"Research Article | Open AccessVolume 5 | Issue 1 |\u00a0https:\/\/doi.org\/10.15228\/2015.v05.i01.p02 Kinetics and Mechanism of Reduction of Fe (III)-Acetohydroxamic Acid by Hydroxylamine Hydrochloride at Acidic pH M. Hassan Department of Chemistry, University of Karachi, Karachi, Pakistan. S. Nisar Department of Chemistry, University of Karachi, Karachi, Pakistan. S. A. 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