{"id":1493,"date":"2013-03-05T23:36:00","date_gmt":"2013-03-05T23:36:00","guid":{"rendered":"https:\/\/chempublishers.sourcingoutfit.com\/?p=1493"},"modified":"2025-06-14T06:55:41","modified_gmt":"2025-06-14T06:55:41","slug":"pjc-0313","status":"publish","type":"post","link":"https:\/\/chempublishers.com\/Pakistan-journal-of-chemistry\/2013\/03\/05\/pjc-0313\/","title":{"rendered":"Piperidine Promoted Regioselective Synthesis of \u03b1, \u03b2-unsaturated Aldehydes"},"content":{"rendered":"\t\t<div data-elementor-type=\"wp-post\" data-elementor-id=\"1493\" class=\"elementor elementor-1493\" data-elementor-post-type=\"post\">\n\t\t\t\t<div class=\"elementor-element elementor-element-5f86670 e-flex e-con-boxed e-con e-parent\" data-id=\"5f86670\" data-element_type=\"container\">\n\t\t\t\t\t<div class=\"e-con-inner\">\n\t\t<div class=\"elementor-element elementor-element-b378445 e-con-full e-flex e-con e-child\" data-id=\"b378445\" data-element_type=\"container\">\n\t\t\t\t<div class=\"elementor-element elementor-element-3fbecff elementor-widget elementor-widget-text-editor\" data-id=\"3fbecff\" data-element_type=\"widget\" data-widget_type=\"text-editor.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t\t\t\t\t<table border=\"0\" width=\"100%\" cellspacing=\"0\" cellpadding=\"0\" align=\"center\">\n<tbody>\n<tr>\n<td>\n<div><strong>Research Article | Open Access<\/strong><\/div>\n<div class=\"item doi\"><span class=\"value\">Volume 3 | Issue 1 | Paper 03 |&nbsp; <a href=\"https:\/\/chempublishers.com\/Pakistan-journal-of-chemistry\/wp-content\/uploads\/sites\/2\/2025\/01\/PJC-v03.i01.p03.pdf\" target=\"_blank\" rel=\"noopener\">https:\/\/doi.org\/10.15228\/2013.v03.i01.p03<\/a><\/span><\/div>\n<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n<article class=\"obj_article_details\">\n<h4>Piperidine Promoted Regioselective Synthesis of \u03b1, \u03b2-unsaturated Aldehydes<\/h4>\n<div class=\"row\">\n<h4 class=\"main_entry\"><span class=\"name\">A.H. Banday<\/span><\/h4>\n<p>Department of Chemistry, Islamia College of Science and Commerce, Srinagar-190009, J&amp;K, India<\/p>\n<table border=\"0\" width=\"93%\" cellspacing=\"0\" cellpadding=\"0\" align=\"center\">\n<tbody>\n<tr>\n<td align=\"center\" valign=\"top\"><strong>Received<\/strong><br>05 Apr, 2013<\/td>\n<td align=\"center\" valign=\"top\"><strong>Accepted<\/strong><br>07 Oct, 2013<\/td>\n<td align=\"center\" valign=\"top\"><strong>Published<\/strong><br>09 Nov, 2013<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n<div class=\"item abstract\">\n<p align=\"justify\">ABSTRACT:<\/p>\n<p class=\"ql-align-justify\">An efficient, facile and regioselective synthesis of \u03b1,\u03b2-unsaturated aldehydes from \u03b2-hydroxynitriles is reported. The reaction is carried out using DIBAL-H and promoted by piperidine under dry conditions at a temperature of -78 oC and can be described as a concomitant reduction-elimination reaction. The same reaction if carried out in the absence of piperidine gives mainly the uneliminated reduction product. The products formed are of immense importance as synthons in a large number of chemical reactions and biological processes.<\/p>\n<\/div>\n<div class=\"item abstract\">\n<div>\n<h3 class=\"label\">How to Cite this paper?<\/h3>\n<div class=\"csl-entry\">\n<p><strong>APA-7 Style<\/strong><br>Banday, A.H. (2013). Piperidine Promoted Regioselective Synthesis of \u03b1, \u03b2-unsaturated Aldehydes.&nbsp;<a href=\"https:\/\/doi.org\/10.15228\/2013.v03.i01.p03\" target=\"_blank\" rel=\"noopener\"><em>Pakistan Journal of Chemistry<\/em>, 3(1), 19-22<\/a>. https:\/\/doi.org\/10.15228\/2013.v03.i01.p03<\/p>\n<p><strong>ACS Style<\/strong><br>Banday, A.H. Piperidine Promoted Regioselective Synthesis of \u03b1, \u03b2-unsaturated Aldehydes.&nbsp;<a href=\"https:\/\/doi.org\/10.15228\/2013.v03.i01.p03\" target=\"_blank\" rel=\"noopener\"><em>Pak. J. Chem.<\/em>&nbsp;2013, 3, 19-22<\/a>. https:\/\/doi.org\/10.15228\/2013.v03.i01.p03<\/p>\n<p><strong>AMA Style<\/strong><br>Banday AH. Piperidine Promoted Regioselective Synthesis of \u03b1, \u03b2-unsaturated Aldehydes.&nbsp;<a href=\"https:\/\/doi.org\/10.15228\/2013.v03.i01.p03\" target=\"_blank\" rel=\"noopener\"><em>Pakistan Journal of Chemistry<\/em>. 2013; 3(1): 19-22<\/a>. https:\/\/doi.org\/10.15228\/2013.v03.i01.p03<\/p>\n<p><strong>Chicago\/Turabian Style<\/strong><br>Banday, A., H.. 2013. &#8220;Piperidine Promoted Regioselective Synthesis of \u03b1, \u03b2-unsaturated Aldehydes&#8221;&nbsp;<a href=\"https:\/\/doi.org\/10.15228\/2013.v03.i01.p03\" target=\"_blank\" rel=\"noopener\"><em>Pakistan Journal of Chemistry<\/em>&nbsp;3, no. 1: 19-22<\/a>. https:\/\/doi.org\/10.15228\/2013.v03.i01.p03<\/p>\n<\/div>\n<\/div>\n<\/div>\n<div class=\"item copyright\">\n<p><a href=\"https:\/\/creativecommons.org\/licenses\/by\/4.0\/\" rel=\"license\"><img decoding=\"async\" src=\"https:\/\/i.creativecommons.org\/l\/by\/4.0\/88x31.png\" alt=\"Creative Commons License\"><\/a><\/p>\n<p>This work is licensed under a&nbsp;<a href=\"https:\/\/creativecommons.org\/licenses\/by\/4.0\/\" rel=\"license\">Creative Commons Attribution 4.0 International License<\/a>.<\/p>\n<\/div>\n<\/div>\n<\/article>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t<div class=\"elementor-element elementor-element-7217e73 e-con-full e-flex e-con e-child\" data-id=\"7217e73\" data-element_type=\"container\">\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t","protected":false},"excerpt":{"rendered":"<p>Research Article | Open Access Volume 3 | Issue 1 | Paper 03 |&nbsp; https:\/\/doi.org\/10.15228\/2013.v03.i01.p03 Piperidine Promoted Regioselective Synthesis of \u03b1, \u03b2-unsaturated Aldehydes A.H. Banday Department of Chemistry, Islamia College of Science and Commerce, Srinagar-190009, J&amp;K, India Received05 Apr, 2013 Accepted07 Oct, 2013 Published09 Nov, 2013 ABSTRACT: An efficient, facile and regioselective synthesis of \u03b1,\u03b2-unsaturated [&hellip;]<\/p>\n","protected":false},"author":2,"featured_media":0,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"_acf_changed":false,"footnotes":""},"categories":[1],"tags":[],"class_list":["post-1493","post","type-post","status-publish","format-standard","hentry","category-uncategorized"],"acf":[],"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v25.1 - https:\/\/yoast.com\/wordpress\/plugins\/seo\/ -->\n<title>Piperidine Promoted Regioselective Synthesis of \u03b1, \u03b2-unsaturated Aldehydes - Pakistan Journal of Chemistry<\/title>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/chempublishers.com\/Pakistan-journal-of-chemistry\/2013\/03\/05\/pjc-0313\/\" \/>\n<meta property=\"og:locale\" content=\"en_US\" \/>\n<meta property=\"og:type\" content=\"article\" \/>\n<meta property=\"og:title\" content=\"Piperidine Promoted Regioselective Synthesis of \u03b1, \u03b2-unsaturated Aldehydes - Pakistan Journal of Chemistry\" \/>\n<meta property=\"og:description\" content=\"Research Article | Open Access Volume 3 | Issue 1 | Paper 03 |&nbsp; https:\/\/doi.org\/10.15228\/2013.v03.i01.p03 Piperidine Promoted Regioselective Synthesis of \u03b1, \u03b2-unsaturated Aldehydes A.H. Banday Department of Chemistry, Islamia College of Science and Commerce, Srinagar-190009, J&amp;K, India Received05 Apr, 2013 Accepted07 Oct, 2013 Published09 Nov, 2013 ABSTRACT: An efficient, facile and regioselective synthesis of \u03b1,\u03b2-unsaturated [&hellip;]\" \/>\n<meta property=\"og:url\" content=\"https:\/\/chempublishers.com\/Pakistan-journal-of-chemistry\/2013\/03\/05\/pjc-0313\/\" \/>\n<meta property=\"og:site_name\" content=\"Pakistan Journal of Chemistry\" \/>\n<meta property=\"article:published_time\" content=\"2013-03-05T23:36:00+00:00\" \/>\n<meta property=\"article:modified_time\" content=\"2025-06-14T06:55:41+00:00\" \/>\n<meta property=\"og:image\" content=\"https:\/\/i.creativecommons.org\/l\/by\/4.0\/88x31.png\" \/>\n<meta name=\"author\" content=\"admin\" \/>\n<meta name=\"twitter:card\" content=\"summary_large_image\" \/>\n<meta name=\"twitter:label1\" content=\"Written by\" \/>\n\t<meta name=\"twitter:data1\" content=\"admin\" \/>\n\t<meta name=\"twitter:label2\" content=\"Est. reading time\" \/>\n\t<meta name=\"twitter:data2\" content=\"2 minutes\" \/>\n<script type=\"application\/ld+json\" class=\"yoast-schema-graph\">{\"@context\":\"https:\/\/schema.org\",\"@graph\":[{\"@type\":\"Article\",\"@id\":\"https:\/\/chempublishers.com\/Pakistan-journal-of-chemistry\/2013\/03\/05\/pjc-0313\/#article\",\"isPartOf\":{\"@id\":\"https:\/\/chempublishers.com\/Pakistan-journal-of-chemistry\/2013\/03\/05\/pjc-0313\/\"},\"author\":{\"name\":\"admin\",\"@id\":\"https:\/\/chempublishers.com\/Pakistan-journal-of-chemistry\/#\/schema\/person\/5f5f92c274f1346d6f53fa7864e00a01\"},\"headline\":\"Piperidine Promoted Regioselective Synthesis of \u03b1, \u03b2-unsaturated Aldehydes\",\"datePublished\":\"2013-03-05T23:36:00+00:00\",\"dateModified\":\"2025-06-14T06:55:41+00:00\",\"mainEntityOfPage\":{\"@id\":\"https:\/\/chempublishers.com\/Pakistan-journal-of-chemistry\/2013\/03\/05\/pjc-0313\/\"},\"wordCount\":245,\"publisher\":{\"@id\":\"https:\/\/chempublishers.com\/Pakistan-journal-of-chemistry\/#organization\"},\"image\":{\"@id\":\"https:\/\/chempublishers.com\/Pakistan-journal-of-chemistry\/2013\/03\/05\/pjc-0313\/#primaryimage\"},\"thumbnailUrl\":\"https:\/\/i.creativecommons.org\/l\/by\/4.0\/88x31.png\",\"inLanguage\":\"en-US\"},{\"@type\":\"WebPage\",\"@id\":\"https:\/\/chempublishers.com\/Pakistan-journal-of-chemistry\/2013\/03\/05\/pjc-0313\/\",\"url\":\"https:\/\/chempublishers.com\/Pakistan-journal-of-chemistry\/2013\/03\/05\/pjc-0313\/\",\"name\":\"Piperidine Promoted Regioselective Synthesis of \u03b1, \u03b2-unsaturated Aldehydes - 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